欢迎访问沈阳真空杂志社 Email Alert    RSS服务

真空 ›› 2021, Vol. 58 ›› Issue (2): 58-61.doi: 10.13385/j.cnki.vacuum.2021.02.12

• 真空应用 • 上一篇    下一篇

真空微波器件用无氧铜零件的真空存贮*

刘燕文1, 赵丽2, 陆玉新3, 田宏1, 石文奇1, 赵恒邦1   

  1. 1.中国科学院空天信息创新研究院,北京 100190;
    2.中国航天科工二院空间工程总体部,北京 100854;
    3.天津交通职业学院,天津 300110
  • 收稿日期:2020-05-10 出版日期:2021-03-25 发布日期:2021-04-09
  • 作者简介:刘燕文(1964-),男,天津人,博士。
  • 基金资助:
    *总装预研基金项目(批准号31512010404-1)、国家自然科学基金项目(批准号:61771454)

Storage of Copper Parts Used in Microwave Vacuum Devices

LIU Yan-wen1, ZHAO Li2, LU Yu-xin3, TIAN Hong1, SHI Wen-qi1, ZHAO Heng-bang1   

  1. 1. Aerospace Information Research Institute, Chinese Academy of Science, Beijing 100190, China;
    2. CASIC Space Engineering Development, Beijing 100854, China;
    3. Tianjin Traffic Vocational Institute, Tianjin 300110, China
  • Received:2020-05-10 Online:2021-03-25 Published:2021-04-09

摘要: 零件存储是真空微波器件制造的基础条件,慢波组件一般存放于真空柜中,存放一段时间后,慢波组件中的螺旋线镀铜表面出现了发黑现象,分析表明螺旋线表面镀铜部位发生了硫化。结合进一步的实验研究和理论分析,真空柜中放置的橡胶制品导致了无氧铜材料表面发黑。在真空状态下,硫是比较容易从橡胶套中升华进入真空柜中的,从而会在真空柜中弥漫大量硫蒸气,这些硫蒸气极易与铜发生化学反应形成Cu2S,因此含硫的橡胶套不宜放入真空柜,并且在真空电子器件中也要防止使用含硫的橡胶制品接触无氧铜零件。

关键词: 真空微波器件, 螺旋线, 无氧铜, 真空存储

Abstract: The storage of metal parts is the basic condition for the microwave vacuum devices. Slow wave components are generally stored in vacuum cabinets. After storage for a period of time, blackening occurs on the copper plating surface of the helix in the slow wave component. The analysis showed that the copper plating on the surface of the helix was vulcanized. Combined with further experimental research and theoretical analysis, the rubber products placed in the vacuum cabinet caused the surface blackening of the copper material. In the vacuum, sulfur is relatively easy to sublimate from the rubber sleeve into the vacuum cabinet, which will diffuse a large amount of sulfur vapor in the vacuum cabinet. These sulfur vapor easily reacts with copper to form Cu2S, so the sulfur-containing rubber sleeve should not be placed in a vacuum cabinet, and the use of sulfur-containing rubber products in vacuum electronic devices should be prevented from contacting copper parts.

Key words: microwave vacuum devices, slow-wave structures of helix, copper, storage

中图分类号: 

  • TN107
[1] LIU Y W, TIAN H, LU Y X.Influences of Diamond Material on Heat Dissipation Capabilities of Helical Slow Wave Structures[J]. IEEE Transactions on Electron Devices. 2019, 66(12): 5321-5326.
[2] 荀涛, 孙晓亮, 樊玉伟, 等. 重频吉瓦级高功率微波源硬管化技术研究, 电子科技大学学报, 2020, 1: 87-91.
[3] 刘燕文, 王小霞, 田宏, 等. 纳米粒子薄膜热电子发射性能[J]. 中国科学信息科学, 2015, 45: 145-156.
[4] 廖复疆. 大功率微波真空电子学技术进展[J]. 电子学报, 2006, 313(3): 513-516.
[5] LIU Y W, TIAN H.The temperature variation of a thermionic cathode during electron emission[J]. Science in China E. 2008, 51(9): 1497-1501.
[6] SHIN Y M, BARNETT L R, GAMZINA D, et al. Terahertz vacuum electronic circuits fabricated by UV lithographic molding and reactive ion etching[J]. Applied Physics Letter.2009, 95(18): 181 505- 1-181 505-3.
[7] SIRIGIRI J R, SHAPRIO M A, TEMKIN R J.High power 140GHz quasi-optical gyrotron travelling wave amplifier[J]. Physics Review letter. 2003, 90(25): 56302-56310.
[8] 刘燕文, 田宏, 韩勇, 等. 支取发射电流对热阴极温度影响的研究[J]. 中国科学E, 2008, (9): 1515-1520.
[9] 刘燕文, 田宏. 空间行波管极高真空的获得与测量[J]. 真空, 2018, 55(5): 25-28.
[10] WANG X X, LIAO X H, ZHAO Q L, et al.Performance of an Oxide cathode prepared from submierometercarbomates[J]. IEEE Transactions on Electron Devices. 2011, 58(9): 3195-3199.
[11] 刘燕文, 田宏, 韩勇, 等. 发射均匀的覆纳米粒子薄膜阴极的研究[J]. 物理学报, 2009, 58: 535-542.
[12] LIU Y W, TIAN H, HAN Y.Study on the emission properties of the impregnated cathode with nanoparticle films[J]. IEEE Transactions on Electron Devices. 2012, 59(12): 3618-3624.
[13] WANG X X, LIU Y W.Preparation and Evaluation of the Ammonium Perrhenate Impregnated Ni Sponge Oxide Cathode[J]. IEEE Transactions on ElectronDevices, 2014, 61(2): 605-610.
[14] 廖复疆, 吴固基. 真空电子技术-军事电子装备的心脏[M]. 北京: 国防工业出版社, 2001: 12.
[15] 刘燕文等, 螺旋线行波管慢波组件散热性能研究进展, 真空科学与技术学报, 2011, 31(4): 424-431.
[16] 肖琰, 天然橡胶硫化胶的热氧老化研究, 西北工业大学, 硕士论文, 2006, 20.
[17] 张以忱, 黄英. 真空材料[M]. 北京: 冶金工业出版社, 2005: 73.
[18] 刘燕文, 王小霞, 陆玉新, 等. 用于电真空器件的金属材料蒸发特性[J]. 物理学报, 2016, 65(63): 068502-1-7.
[19] KOHL W H.Materials technology for electron tubes[M]. New York: ReinholdPublishing Corporation, 1951: 162.
[1] 张骁, 刘招贤, 孟冬辉, 任国华, 王莉娜, 闫荣鑫. 多孔石墨烯渗氦仿真研究*[J]. 真空, 2021, 58(1): 10-14.
[2] 刘燕文, 田宏, 陆玉新, 石文奇, 朱虹, 李芬, 李云, 谷兵, 王小霞. 用于微波真空电子器件的光电阴极*[J]. 真空, 2019, 56(6): 7-11.
[3] 刘燕文, 孟宪展, 田 宏, 李 芬, 石文奇, 朱 虹, 谷 兵, 王小霞 . 空间行波管极高真空的获得与测量[J]. 真空, 2018, 55(5): 25-28.
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
No Suggested Reading articles found!