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VACUUM ›› 2023, Vol. 60 ›› Issue (4): 60-64.doi: 10.13385/j.cnki.vacuum.2023.04.11

• Vacuum Acquisition System • Previous Articles     Next Articles

High-precision Measurement Device for Outgassing Rate of Vacuum Materials

LI Jin-ming1,2, WANG Jin-wei1,2, LIU Jun-nan1,2, CHEN Ming1,2   

  1. 1. Shanghai Advanced Research Institute, Chinese Academy of Sciences, Shanghai 201204, China;
    2. Shanghai Synchrotron Radiation Facility, Shanghai 201204, China
  • Received:2022-12-14 Online:2023-07-25 Published:2023-07-26

Abstract: This paper introduces a set of high-precision measuring device for the outgassing rate of vacuum materials based on the method of switching between two pumping paths developed by the engineering machinery vacuum auxiliary laboratory of SSRF Ⅱ beamline project. Based on this method, the outgassing rate of common oxygen free copper material samples in the synchrotron radiation vacuum system was tested. The outgassing amount of the sample with background and the background in the conditions of different temperature, outgassing time,and after the gas path conversion was measured and caculated. The results show that the oxygen free copper outgassing rate is 3.06×10-12Pa·m3·s-1·cm-2 after 72h baking at 150℃, it indicates that the device has a high test accuracy of outgassing rate which can meet the measurement requirements of synchrotron radiation device for the outgassing rate of ultra-high vacuum materials.

Key words: vacuum material, outgassing rate, SPP method

CLC Number:  TB74

[1] 麦振洪. 同步辐射光源及其应用(上册)[M]. 北京: 科学出版社, 2013.
[2] 陈明, 刘俊男, 刘腾飞, 等. 上海光源光束线真空系统[C]//第八届华东三省一市真空学术交流会论文集. 2013: 306-310.
[3] 达道安. 真空设计手册[M]. 3版. 北京: 国防工业出版社, 2004: 1040-1083
[4] SCHINDLER N, EDELMANN C, SCHLEUSSNER D.Measurements of partial outgassing rates[J]. Vacuum, 1996, 47(4): 351-355.
[5] GARKE B, EDELMANN C, GÜNZEL R, et al. Modification of the outgassing rate of stainless steel surfaces by plasma immersion ion implantation[J]. Surface & Coatings Technology, 1997, 93(2/3): 318-326.
[6] SAITO K, SATO Y, INAYOSHI S, et al.Measurement system for low outgassing materials by switching between two pumping paths[J]. Vacuum, 1996, 47(6-8): 749-752.
[7] 曾祥坡, 张涤新, 冯焱, 等. 小孔流导法测量材料放气率研究[J]. 真空, 2010, 47(3): 55-58.
[8] 冯焱, 曾祥坡, 张涤新, 等. 小孔流导法材料放气率测量装置的设计[J]. 宇航计测技术, 2010, 30(3): 66-69.
[9] 张涤新, 曾祥坡, 冯焱, 等. 材料放气率测量方法评述[J]. 真空, 2010, 47(6): 1-5.
[10] 董猛, 冯焱, 成永军, 等. 材料在真空环境下放气的测试技术研究[J]. 真空与低温, 2014(1): 46-51.
[11] 冯焱, 董猛, 吴晓斌, 等. 基于分压力测量的真空材料放气率测试方法研究[J]. 真空, 2013, 50(4): 49-52.
[12] 冯焱, 董猛, 成永军. 橡胶材料在真空环境下的放气性能研究[C]//中国真空学会2014学术年会论文摘要集. 2014: 151-156.
[13] 董猛, 冯焱, 盛学民, 等. 双通道气路转换法材料放气率测试研究[C]//中国真空学会2012学术年会论文摘要集. 2012: 107.
[14] WANG L, YAN R X, SUN L C.Outgassing analysis of ultra-high vacuum facility[J]. Spacecraft Environment Engineering, 2009, 26(2): 158-161
[15] 汪力, 孙立臣, 闫荣鑫, 等. 超高真空环境下测试产品的放气分析[J]. 航天器环境工程, 2010, 27(6): 735-738.
[16] 孙立臣, 童靖宇, 汪力, 等. 环模设备研制用玻璃钢的放气性能研究[J]. 航天器环境工程, 2007, 24(2): 104-108.
[17] 罗艳, 王魁波, 吴晓斌, 等. 高精度真空材料放气测试研究[J]. 真空科学与技术学报, 2016, 36(3): 251-257.
[18] 罗艳, 王魁波, 吴晓斌, 等. 电镀件的真空放气特性研究[J]. 真空科学与技术学报, 2022, 42(8): 578-583.
[19] FENG Y, DONG M, LI D, et al.Study on vacuum materials outgassing rate using the method of switching between two pumping paths[J]. Mapan: Journal of Metrology Society of India, 2014, 29(4): 229-234.
[20] 张以忱, 黄英. 真空材料[M]. 北京: 冶金工业出版社, 2005.
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