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VACUUM ›› 2021, Vol. 58 ›› Issue (2): 10-14.doi: 10.13385/j.cnki.vacuum.2021.02.03

• Thin Film • Previous Articles     Next Articles

Effects of Modulation Ratio on Mechanical Properties of Cr/TiN Nano-multilayers Prepared by Arc Ion Plating

WU Yan-chao, LIU Yu-yao, LIU Yang, GAO Sheng-yuan, HUANG Mei-dong   

  1. College of Physics and Materials Science, Tianjin Normal University, Tianjin 300387, China
  • Received:2020-12-02 Online:2021-03-25 Published:2021-04-09

Abstract: Cr/TiN nanoscale multilayers were deposited by arc ion plating with different modulation ratios. The surface morphology, microstructure, hardness and adhesion strength to the substrate of the multilayers were investigated by SEM, AFM, XRD and nano-indenter, respectively. The results show that the Cr/TiN nano-multilayers have compact microstructure with smooth surfaces and comprehensively excellent mechanical properties, indicating nano-interface effects exist in the films. The maximum hardness of 33.22GPa was achieved as the modulation ratio of 2∶3 was applied.

Key words: arc ion plating, Cr/TiN nano-multilayers, hardness, modulation ratio

CLC Number: 

  • TB79
[1] LI D J, KANG Y B, DONG L, et al.Influence of modulation ratio on structure and properties of nanoscale ZrB2/ZrAlN multilayered coatings[J]. Science China-Technological Sciences, 2010, 53(3): 772-775.
[2] 李红, 徐保珍, 侯金宝, 等. 纳米多层膜及其在材料连接应用中的研究进展[J]. 航空制造技术, 2019, 62(12): 14-21.
[3] WANG Y, WU B H, JIANG F, et al.Microstructure and mechanical properties of Cr films deposited with different peak powers by high-power impulse magnetron sputtering[J]. Rare Metals, 2017.
[4] FU C F, CHEN X M, LI L, et al.Effects of the Cr doping on structure and optical properties of ZnO thin films[J]. Optoelectronics Letters, 2010, 6(1): 37-40.
[5] 王飞飞, 何乃如, 吉利, 等. Cr/Cr2O3多层薄膜的制备、力学及摩擦学性能研究[J]. 摩擦学学报, 2016, 36(2): 226-232.
[6] BALAKRISHNAN G, SASTIKUMAR D, KUPPUSAMI P, et al.Microstructural and mechanical properties of Al2O3/ZrO2 nanomultilayer thin films prepared by pulsed laser deposition[J]. Applied Physics A-Materials Science & Processing, 2018, 124(2).
[7] LIU M Y, TAN M, LIU G Q, et al.The effects of modulation period, modulation ratio,and deposition temperature on microstructure and mechanical properties of ZrB2/W multilayers[J]. Science China-Technological Sciences, 2010, 53(9): 2350-2354.
[8] WEI Y Q, ZONG X Y, JIANG Z Q, et al.Characterization and mechanical properties of TiN/TiAlN multilayer coatings with different modulation periods[J]. International Journal of Advanced Manufacturing Technology, 2018, 96(5-8): 1677-1683.
[9] 阎红娟, 田沁叶, 刘峰斌, 等. 调制周期对TaN/TiSiN纳米多层膜微观结构与性能影响[J]. 热喷涂技术, 2019, 11(4): 25-30.
[10] 刘闯, 周晖, 张凯锋, 等. 调制比对磁控溅射Ti/TiN多层膜组织结构和结合力的影响[J]. 电镀与涂饰, 2019, 38(5): 212-217.
[11] 崔文芳, 曹栋, 秦高悟. 磁控溅射沉积Ti/TiN多层膜的组织特征及耐磨损性能[J]. 金属学报, 2015, 51(12): 1531-1537.
[12] 戴剑锋, 史鑫, 吴贵智, 等. 多弧离子镀沉积 Ti/TiN 多层膜的力学和摩擦学性能[J]. 兰州理工大学学报, 2018, 44(2): 169-172.
[13] SHANAGHI A, GHASEMI S, CHU P K, et al.Effect of Ti interlayer on corrosion behavior of nanostructured Ti/TiN multilayer coating deposited on TiAl6V4[J]. Materials and Corrosion, 2019, 70(11): 2113-2127.
[14] ZHAO Y H, LIN G Q, XIAO J Q, et al.Ti/TiN multilayer thin films deposited by pulse biased arc ion plating[J]. Applied Surface Science, 2011, 257(7): 2683-2688.
[15] ZHANG Q, LENG Y X, QI F, et al.Mechanical and corrosive behavior of Ti/TiN multilayer films with different modulation periods[J]. Nuclead Instruments & Methods In Physcis Research Section B-Beam Interactions With Materials and Atoms, 2007, 257: 411-415.
[16] 车德良. 多弧离子镀氮化物薄膜的性能及应用[D]. 大连: 大连理工大学, 2005.
[17] 蔡志海, 牛庆银, 底月兰, 等. 调制周期对Cr/CrN纳米多层膜的结构与性能的影响[J]. 金属热处理, 2011, 36(1): 29-32.
[18] ZHAO J P, WANG X, CHEN Z Y, et al.Overall energy model for preferred growth of TiN films during filtered arc deposition[J]. Journal of Physics D—Applied Physics, 1997, 30(1): 5-12.
[19] 龚海飞, 邵天敏, 张晨辉, 等. TiN/Ti多层膜调制比对摩擦磨损行为影响的研究[J]. 无机材料学报, 2008, 23(4): 758-762.
[20] 郑晓华, 林玲玲, 常新新, 等. 调制比对磁控溅射法生长DLC/WSx多层膜微结构和力学性能的影响[J]. 中国有色金属学报, 2018, 28(7): 1343-1350.
[21] 肖娜, 杜菲菲, 杨波. 调制周期对TiN/Ti多层膜组织结构和结合力的影响[J]. 中国表面工程, 2015, 28(2): 65-69.
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