欢迎访问沈阳真空杂志社 Email Alert    RSS服务

VACUUM ›› 2020, Vol. 57 ›› Issue (3): 17-20.doi: 10.13385/j.cnki.vacuum.2020.03.04

• Thin Film • Previous Articles     Next Articles

Effect of Sputtering Power on Microstructure of Er Thin Films Deposited by Magnetron Sputtering

ZHANG Qing-fang1,2, YI Yong1, LUO Jiang-shan2   

  1. 1. School of Material Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China;
    2. Research Center of Laser Fusion, China Academy of Engineering Physics, Mianyang 621900, China
  • Received:2019-12-19 Published:2020-06-18

Abstract: A series of erbium(Er) films were deposited by DC magnetron sputtering method. The effect of sputtering power on the microstructure of the Er thin films was investigated by X-ray diffraction and scanning electron microscope. The experimental results show that all the Er films deposited with the sputtering power of 20W~60W are mainly composed of hcp phase, and present(110) preferred orientation obviously. The Er films grow with typical columnar crystals that increase accordingly with the increasing of sputtering power. The Er films are dense and flat with the average grain size of 7.7nm~9.6nm and surface roughness of 2.1nm. The Er films deposited by magnetron sputtering exhibit different microstructural characteristics from other Er films grown by electron beam vapor.

Key words: magnetron sputtering, Er thin film, microstructure, preferred orientation

CLC Number: 

  • TB742
[1] Dow P A, Briers G W, Dewey M A P, et al. The structure of erbium deuteride targets for neutron generators[J]. Nuclear Instruments and Methods, 1968, 60(3); 293-296.
[2] Banerjee A, Abhilash S R, Umapathy G R, et al.Material engineering to fabricate rare earth erbium thin films for exploring nuclear energy sources[J]. Nuclear Instruments and Methods in Physics Research, A, 2018, 887: 34-39.
[3] Brumbach M T, Ohlhausen J A, Zavadil K R, et al.Activation of erbium films for hydrogen storage[J]. Journal of Applied Physics, 2011, 109: 114911.
[4] Ciria M, Arnaudas J I, Moral A D.Magnetoelastic properties of epitaxial holmium and erbium thin films[J]. Applied Physics Letters, 1998, 72(16); 2044-2046.
[5] Witt J D S, Cooper J F K, Satchell N, et al. Magnetic phases of sputter deposited thin-film erbium[J]. Scientific Reports, 2016, 6: 39021.
[6] Shen H H, Peng S M, Long X G, et al.Effect of thermal annealing on the microstructure and morphology of erbium films[J]. Thin Solid Films, 2012, 520: 6196-6200.
[7] Gu E D, Savaloni H, Player M A, et al.Characterization of evaporated erbium films at various stages of growth[J]. Journal of Physical and Chemistry of Solids, 1992, 53(1): 127-136.
[8] Savaloni H, Player M A.Influence of deposition conditions and of substrate on the structure of UHV deposited erbium films[J]. Vacuum, 1995, 46(2): 167-179.
[9] Shen H H, Peng S M, Long X G, et al.The effect of substrate temperature on the oxidation behavior of erbium thick films[J]. Vacuum, 2012, 86: 1097-1101.
[10] Shen H H, Peng S M, Long X G, et al.Influence of growth parameters on the microstructures of erbium films deposited on Si(111)substrates[J]. Vacuum, 2012, 86: 2075-2081.
[11] Parish C M, Snow C S, Kammler D R, et al.Processing effects on microstructure in Er and ErD2 thin-films[J]. Journal of Nuclear Materials, 2010, 403: 191-197.
[12] Dakhel A A.Characterisation of oxidised erbium films deposited on Si(100)substrates[J]. Materials Chemistry and Physics, 2006, 100: 366-371.
[13] 谢华, 罗江山, 黎军, 等. 纳米晶Cu薄带的单辊法制备及结构分析[J]. 强激光与粒子束, 2006, 18(10): 1639-1642.
[14] Klug H P, Alexander L E.X-ray diffraction procedure for polycrystalline and amorphous materials[M]. New York; John Wiley and Son, 1974: 643-655.
[1] WANG Xiao-ming, E Dong-mei, WU Jun-sheng, ZHANG Xu-yue, ZHOU Yan-wen. Simulation of MagnetronSputtering Enhancement Based on Plasma [J]. VACUUM, 2020, 57(3): 5-6.
[2] FANG Bo, ZHANG Lin, CAI Fei, ZHANG Shi-hong. Study on Wear Properties of Duplex-Treated CrVN Composite Coatings by Plasma Nitriding and Arc Ion Plating [J]. VACUUM, 2020, 57(2): 33-39.
[3] WU Hou-pu, TIAN Qin-wen, TIAN Xiu-bo, GONG Chun-zhi. Development and Discharge Behavior of Novel Double Bipolar Pulse High Power Impulse Magnetron Sputtering System [J]. VACUUM, 2019, 56(6): 1-6.
[4] LIAO Rong, DENG Yong-jian, WANG Jia-ju, ZHAO Fei-lan, ZHENG Ruo-qian, LIU Hui-jun, KE Jia-chong. Preparation and Properties of High Dielectric Hafnium Oxide Thin Film [J]. VACUUM, 2019, 56(5): 52-55.
[5] WU Shi-cai, SHANG Xin-de. Application of Flexible Coating Materials in Circuit Board Industry [J]. VACUUM, 2019, 56(5): 65-68.
[6] LUO Jun-yao, LIU Guang-zhuang, YANG Zhao, LI Bao-chang, TA Shi-wo. Study on Magnetron Sputtering and Wet Etching Technology of Chromium Silicon Thin Film Resistive Layer [J]. VACUUM, 2019, 56(5): 61-64.
[7] WU Xing, JIANG Ai-hua, CHENG Yong. Effect of RF Power on Structure and Mechanical Properties of DLC Films [J]. VACUUM, 2019, 56(4): 34-36.
[8] WANG Huai-qian, JIANG Hong-wei. TiN Nano-Thin Films Prepared by Magnetron Sputtering Reaction [J]. VACUUM, 2019, 56(4): 37-39.
[9] LIU Chan, WANG Dong-wei, LI Xiao-min, WU Ying-tong, HUANG Mei-dong. Influence of pulsed negative bias on structure and properties of carbon films grown by magnetron sputtering [J]. VACUUM, 2019, 56(2): 69-73.
[10] WANG Fu-zhen, CHEN Da-min, YAN Yuan-quan. The cleaning sources with argon ions using vacuum arc discharge technology [J]. VACUUM, 2019, 56(1): 27-33.
[11] WANG Xiao-ran, MA Yan-bin, DUAN Ping, LI Ru-yong, ZHUANG Bi-hui, CUI Min, YUAN An-juan, DENG Jin-xiang. Effect of Mg doping concentration on Ga2O3 thin films prepared by RF magnetron sputtering [J]. VACUUM, 2018, 55(6): 68-72.
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
[1] LI De-tian, CHENG Yong-jun, ZHANG Hu-zhong, SUN Wen-jun, WANG Yong-jun, SUN Jian, LI Gang, . Preparations and applications of carbon nanotube field emitters[J]. VACUUM, 2018, 55(5): 1 -9 .
[2] ZHOU Bin-bin, ZHANG jian, HE Jian-feng, DONG Chang-kun. Carbon nanotube field emission cathode based on direct growth technique[J]. VACUUM, 2018, 55(5): 10 -14 .
[3] LI Zhi-sheng. Development of ultra large shielded door for infrared calibration in simulated space environment[J]. VACUUM, 2018, 55(5): 66 -70 .
[4] ZHENG Lie, LI Hong. Design of 200kV/2mA continuous adjustable DC high voltage generator[J]. VACUUM, 2018, 55(6): 10 -13 .
[5] CHAI Xiao-tong, WANG Liang, WANG Yong-qing, LIU Ming-kun, LIU Xing-zhou, GAN Shu-yi. Operating parameter data acquisition system for single vacuum pump based on STM32F103 microcomputer[J]. VACUUM, 2018, 55(5): 15 -18 .
[6] SUN Li-zhi, YAN Rong-xin, LI Tian-ye, JIA Rui-jin, LI Zheng, SUN Li-chen, WANG Yong, WANG Jian, . Research on distributing law of Xenon in big accumulation chamber[J]. VACUUM, 2018, 55(5): 38 -41 .
[7] HUANG Si, WANG Xue-qian, MO Yu-shi, ZHANG Zhan-fa, YING Bing. Experimental study on similarity law of liquid ring compressor performances[J]. VACUUM, 2018, 55(5): 42 -45 .
[8] JI Ming, SUN Liang, YANG Min-bo. Design of automatic sealing and locking scheme for lunar sample[J]. VACUUM, 2018, 55(6): 24 -27 .
[9] LI Min-jiu, XIONG Tao, JIANG Ya-lan, HE Yan-bin, CHEN Qing-chuan. 20kV high voltage based on double transistor forward converter pulse power supply for metal deburring[J]. VACUUM, 2018, 55(5): 19 -24 .
[10] LIU Yan-wen, MENG Xian-zhan, TIAN Hong, LI Fen, SHI Wen-qi, ZHU Hong, GU Bing. Test of ultra high vacuum in space traveling-wave tube[J]. VACUUM, 2018, 55(5): 25 -28 .