欢迎访问沈阳真空杂志社 Email Alert    RSS服务

VACUUM ›› 2021, Vol. 58 ›› Issue (4): 21-24.doi: 10.13385/j.cnki.vacuum.2021.04.04

• Thin Film • Previous Articles     Next Articles

Effect of RF Power and Sputtering Pressure on Al Film Sputtered on Polythylene Terephthalate Substrates

ZHANG Jian, NIU Xia-bin, LI Jian-hao, QI Zhen-hua   

  1. School of Mechanica and Power Engineering, Shenyang University of Chemical Technology Shenyang, 110142, China
  • Received:2020-09-30 Online:2021-07-25 Published:2021-08-05

Abstract: Aiming at the traditional aluminum production technology, in order to improve the adhesion and barrier property of the film, the RF magnetron sputtering aluminum plating process was adopted to prepare the high barrier layer of pure aluminum by depositing pure aluminum on the surface of PET plastic film. The influences of RF power and sputtering air pressure on film adhesion and barrier property were investigated by changing the parameters of RF power and sputtering air pressure. The results show that the RF power and sputtering pressure in the deposition process have a great influence on the performance of the magnetron sputtered Al film. Under a certain sputtering pressure, the bonding strength of the film layer gradually increases with the increase of the RF power, and the barrier property of the film layer increases with the increase of the RF power, and then decreases. When the RF power is 85W, the minimum oxygen transmittance is 1.11cm3/(m2·day·atm). Under the condition of the same RF power, the binding force increases first and then decreases with the increase of sputtering air pressure, and the barrier property of the film decreases gradually with the increase of sputtering air pressure. When the sputtering pressure was 0.5Pa, the highest binding force was 1.68N/mm. Compared with the traditional aluminum film, the binding force is increased by 2 times and the barrier property is increased by 5 times.

Key words: Al, high barrier materials, RF magnetron sputtering, RF power, sputtering pressure

CLC Number: 

  • TB34
[1] 丁泽良, 孙敏, 王文韬. 溅射工艺参数对SiO2/PET包装膜结合强度的影响[J]. 包装学报, 2013, 5(2): 26-29.
[2] 刘盛友, 刘长松, 程千会. Al2O3超疏水薄膜的制备及其耐腐蚀性研究[J]. 表面技术, 2017, 46(12): 238-244.
[3] KIM P, KREDER M J, ALVARENGA J, et al.Hierarchical or not? Effect of the length scale and hierarchy of the surface roughness on omniphobicity of lubricant infused substrates[J]. Nano letters, 2013, 13(4): 1793.
[4] 朱雪婷, 孙勇, 郭中正, 等. 射频磁控溅射沉积Al/Al2O3纳米多层膜的结构及性能[J]. 真空科学与技术学报, 2013, 24(5): 477-482.
[5] FERMEGLIA M, COSOLI P, FERRONE M, et al.PET/PEN blends of industrial interest as barrier materials. Part I. Many-scale molecular modeling of PET/PEN blends[J]. Polymer, 2006, 47(16): 5979-5989.
[6] LANGE J, WYSER Y.Recent innovations in barrier technologies for plastic packaging-a review[J]. Packaging Technology and Science, 2003, 16(4): 149-158.
[7] 林长生. SiO2/Al2O3/PET复合膜的制备及其透湿性能研究[D]. 株洲: 湖南工业大学, 2015.
[8] 彭丽平, 王兆松, 李剑锋, 等. 铝基复合材料表面多层复合厚膜的研究[J]. 真空科学与技术学报, 2010, 25(5): 505-509.
[9] 潘健, 叶青松, 胡国利. 蒸镀氧化铝/氧化硅型高阻隔性包装薄膜[J]. 塑料包装, 2018, 28(2): 20-22.
[10] GALDI M R, INCARNATO L.Influence of composition on structure and barrier properties of active PET films for food packaging applications[J]. Packaging Technology and Science, 2011, 24(2): 89-102.
[11] 孙宝玉, 巴德纯, 段永利, 等. 真空热处理对镀Al薄膜NdFeB磁体组织和耐蚀性的影响[J]. 真空科学与技术学报, 2011(2): 221-224.
[12] FAVARO M, ZANAZZI E, PATELLI A, et al.Aluminum doped zinc oxide coatings at low temperature by atmospheric pressure plasma jet[J]. Thin Solid Films, 2020, 708(2): 1-7.
[13] STRULLER C F, KELLY P J, COPELANDB N J.Aluminum oxide barrier coatings on polymer films for food packaging applications[J]. Surf Coat Tech, 2014, 241(3): 130-137.
[14] 霍纯青, 陈强, 孙运金, 等. 磁控溅射制备硅铝阻隔膜的研究[J]. 包装工程, 2007, 28(8): 40-42.
[15] 林晶, 刘壮, 孙智慧, 等. 负偏压对PET上磁控溅射氧化铝薄膜的影响[J]. 真空科学与技术学报, 2009, 29: 91-93.
[1] YU Jin-jun, DO Xin, LIU Min-qiang. Design of a Compound Molecular Pump With Ultra-high Vacuum and High Pumping Speed [J]. VACUUM, 2021, 58(4): 36-41.
[2] FU Xue-cheng, XU Jin-bin, WU Li-ying, HUANG Sheng-li, WANG Ying. Study on Uniformity of Inclined Magnetron Sputtering with Small Circular Plane Target [J]. VACUUM, 2021, 58(4): 1-5.
[3] JI Jian-chao, YAN Yue, HA En-hua. Study Progress of AZO Films by Sol-gel Methods [J]. VACUUM, 2021, 58(4): 30-35.
[4] LI Jing, TAN Zhang-hua, LIU Xing-xing, CHEN Ying-lin, LI Hao-wen, YANG Hao, WANG Chang-lin, WANG Jiang-yong, XU Cong-kang. Quantitative Analysis of AES Depth Profiles for Ni/Cr Multilayered Film by Genetic Algorithms [J]. VACUUM, 2021, 58(4): 6-11.
[5] BAI Ming-yuan, WANG Xin, ZHEN Zhen, MU Ren-de, HE Li-min, XU Zhen-hua. Phase Stability and Interfacial Bonding Strength of Rare Earth Zirconate Novel Thermal Barrier Coatings [J]. VACUUM, 2021, 58(4): 12-20.
[6] REN Shao-peng, GAO Peng, WANG Rui-sheng, JIN Xiu, WANG Zhong-lian, ZHANG Yi. Introduction for the Standard of Interference Filters Used for Fluorescence Detection Analysis [J]. VACUUM, 2021, 58(4): 25-29.
[7] XU Li, WU Ze-ming, LIU Xu, LI hao. Boiler Temperature Control System Based on Fuzzy Neural Network [J]. VACUUM, 2021, 58(4): 77-80.
[8] QI Da-wei, LI Wei-hua, LI Chuan-xu, WU Bin, CHEN De-jiang, TANG Zhi-gong. Pneumatic Design of Centrifugal Vacuum Pump for Large Wind Tunnel [J]. VACUUM, 2021, 58(4): 49-53.
[9] ZHENG Xia, GUAN Feng-ping, WEN Li-pong, JI Lu-yu, XING Jian-sheng, XIE Huai-dong. Design and Research of Beam Measuring Device for 230 MeV Superconducting Cyclotron [J]. VACUUM, 2021, 58(4): 54-57.
[10] XIE Yong-qiang, JIN Li-yan, YANG Xiao-dong, WANG Cheng-jun, XIA Dan, SU Chun. Finite Elements Analysis and Optimal Design for the Temperature Field of Vacuum Brazing Furnace [J]. VACUUM, 2021, 58(4): 58-62.
[11] MA Yi-Gang, LI Zhi-hui. Application of Ultra-high and High Vacuum Technology [J]. VACUUM, 2021, 58(4): 98-102.
[12] YANG Guang, LIU Huan, WANG Ding-ding, LUO Li-ping, LV Xu-ming, QI Yang. Effect of Crack in Micrometer Scale on the Water-cooled Oxygen-free Copper Crucible [J]. VACUUM, 2021, 58(4): 81-86.
[13] TU Jun, SONG Wen-jie, ZHANG Bin, YU De-ping, LI Yi-hong. Experimental Study on the Working Characteristics of Steam Plasma Torch [J]. VACUUM, 2021, 58(4): 87-92.
[14] ZHANG Long-he. Analysis and Treatment of Common Faults of Oil Sealed Rotary Vacuum Pump [J]. VACUUM, 2021, 58(3): 17-22.
[15] LUO Jun-wen. Development of Large-Scale Metal Coil Surface Modification Continuous Roll to Roll Coating Production Line [J]. VACUUM, 2021, 58(3): 35-38.
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
[1] LI De-tian, CHENG Yong-jun, ZHANG Hu-zhong, SUN Wen-jun, WANG Yong-jun, SUN Jian, LI Gang, . Preparations and applications of carbon nanotube field emitters[J]. VACUUM, 2018, 55(5): 1 -9 .
[2] ZHOU Bin-bin, ZHANG jian, HE Jian-feng, DONG Chang-kun. Carbon nanotube field emission cathode based on direct growth technique[J]. VACUUM, 2018, 55(5): 10 -14 .
[3] LI Zhi-sheng. Development of ultra large shielded door for infrared calibration in simulated space environment[J]. VACUUM, 2018, 55(5): 66 -70 .
[4] ZHENG Lie, LI Hong. Design of 200kV/2mA continuous adjustable DC high voltage generator[J]. VACUUM, 2018, 55(6): 10 -13 .
[5] CHAI Xiao-tong, WANG Liang, WANG Yong-qing, LIU Ming-kun, LIU Xing-zhou, GAN Shu-yi. Operating parameter data acquisition system for single vacuum pump based on STM32F103 microcomputer[J]. VACUUM, 2018, 55(5): 15 -18 .
[6] SUN Li-zhi, YAN Rong-xin, LI Tian-ye, JIA Rui-jin, LI Zheng, SUN Li-chen, WANG Yong, WANG Jian, . Research on distributing law of Xenon in big accumulation chamber[J]. VACUUM, 2018, 55(5): 38 -41 .
[7] HUANG Si, WANG Xue-qian, MO Yu-shi, ZHANG Zhan-fa, YING Bing. Experimental study on similarity law of liquid ring compressor performances[J]. VACUUM, 2018, 55(5): 42 -45 .
[8] JI Ming, SUN Liang, YANG Min-bo. Design of automatic sealing and locking scheme for lunar sample[J]. VACUUM, 2018, 55(6): 24 -27 .
[9] LI Min-jiu, XIONG Tao, JIANG Ya-lan, HE Yan-bin, CHEN Qing-chuan. 20kV high voltage based on double transistor forward converter pulse power supply for metal deburring[J]. VACUUM, 2018, 55(5): 19 -24 .
[10] LIU Yan-wen, MENG Xian-zhan, TIAN Hong, LI Fen, SHI Wen-qi, ZHU Hong, GU Bing. Test of ultra high vacuum in space traveling-wave tube[J]. VACUUM, 2018, 55(5): 25 -28 .