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VACUUM ›› 2021, Vol. 58 ›› Issue (6): 21-26.doi: 10.13385/j.cnki.vacuum.2021.06.04

• Thin Film • Previous Articles     Next Articles

Nano Film Deposition Technology Based on Magnetron Sputtering

ZHU Bei-bei1, NI Chang2, QIN Lin1, CHU Jian-ning2, CHEN Xiao2, XU Jian-feng2   

  1. 1. Shanghai Institute of Aerospace Control Technology, Shanghai 201109, China;
    2. School of Mechanical Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074, China
  • Received:2020-11-18 Online:2021-11-25 Published:2021-11-30

Abstract: The metallization coating of the hemispherical resonator is an important process in the development of the hemispherical resonator gyroscope. For the requirement of maintaining a high Q value after the metallization of the hemispherical resonator, the high-precision preparation of nano metal films is required. In this paper, nano aluminum films were prepared on quartz glass substrates by DC magnetron sputtering with high purity Al as target material and high purity Ar as sputtering gas. The thickness, surface roughness and surface morphology of the films deposited under different sputtering power and chamber pressure were measured and characterized. The effects of process parameters on deposition rate, surface roughness and micro morphology of the Al films were discussed. The results show that the deposition rate of Al films increases with the increase of sputtering power. With the increase of chamber pressure, the deposition rate shows a trend of first increasing and then decreasing. With the increase of sputtering power, the grain size of the films increases, and with the increase of the chamber pressure, the particle diameter of the film increases first and then decreases. The as-coated film was the most uniform and compact under the condition of 100W sputtering power and 1.6Pa chamber pressure. The above conclusions have important guiding significance for the high-quality preparation of hemispherical harmonic oscillator curved nano films.

Key words: magnetron sputtering, hemispherical resonator, nano film, sputtering power, chamber pressure

CLC Number: 

  • O484.1
[1] ROZELLE D M.The hemispherical resonator gyro: From wineglass to the planets[J]. Advances in the Astronautical Sciences, 2009, 134: 1157-1178.
[2] MARIO N A, CATERINA C, FRANCESCO D, et al.Advanced in gyro-scope technologies[M]. Berlin: Springer, 2013: 1-30.
[3] SHKEL A M.Type I and type II micromachined vibratory gyroscopes[C]//2006 IEEE/ION Position, Location, and Navigation Symposium. IEEE, 2006.
[4] KANIK M, BORDEENITHIKASEM P, Kim D, et al.Metallic glass hemispherical shell resonators[J]. Journal of Microelectromechanical Systems, 2015, 24(1): 19-28.
[5] 宝音贺西, 马鹏斌. 火星探测器自主导航方法综述[J]. 飞控与探测, 2018, 1(1): 34-40.
[6] WANG X, WU W, LOU B, et al.The modeling of hemispherical resonator gyro and its space applications[C]//International Symposium on Precision Engineering Measurements & Instrumentation. International Society for Optics and Photonics, 2011.
[7] JEANROY A, GROSSET G, GOUDON J C, et al.HRG by Sagem from laboratory to mass production[C]//IEEE International Symposium on Inertial Sensors & Systems. IEEE, 2016.
[8] NAGOURNEY T, CHO J Y, DARVISHIAN A, et al.Effect of metal annealing on the Q-factor of metal-coated fused silica micro shell resonators[C]//IEEE International Symposium on Inertial Sensors & Systems. IEEE, 2015.
[9] GINER J, VALDEVIT L, SHKEL A M.Glass-blown pyrex resonator with compensating Ti coating for reduction of TCF[M]. 2014.
[10] DEMENKOV N P, TRAN D M.Fuzzy description hemispherical resonator gyro error[J]. Procedia Computer Science, 2019, 150: 88-94.
[11] SHAO P, TAVASSOLI V, MAYBERRY C L, et al.A 3D-harpss polysilicon microhemispherical shell resonating gyroscope: Design, fabrication, and characterization[J]. IEEE Sensors Journal, 2015, 15(9): 4974-4985.
[12] ZHOU X, WU Y L, XIAO D B, et al.An investigation on the ring thickness distribution of disk resonator gyroscope with high mechanical sensitivity[J]. International Journal of Mechanical Sciences, 2016, 117: 174-181.
[13] HUO Y, REN S Q, YI G X, et al.Motion equations of hemispherical resonator and analysis of frequency split caused by slight mass non-uniformity[J]. Chinese Journal of Aeronautics, 2020, 33(10): 2660-2669.
[14] 张挺, 徐思宇, 冒继明, 等. 半球陀螺谐振子的金属化镀膜工艺技术研究[J]. 压电与声光, 2006(5): 538-540.
[15] 杜晓松, 李杰, 蒋亚东, 等. 离轴溅射法中最佳几何参量的预测[J]. 真空, 2007(3): 5-8.
[16] 李维源, 朱蓓蓓, 孙权权, 等. 基于电子束蒸发沉积的曲面纳米薄膜均匀性研究[J]. 飞控与探测, 2019, 2(2): 64-70.
[17] 陈国良, 郭太良. 直流磁控溅射制备铝薄膜的工艺研究[J]. 真空, 2007(6): 39-42.
[18] 成都电讯工程学院. 气体放电及离子管[M]. 北京: 人民教育出版社, 1961, 107.
[19] KUMRU M.A comparison of the optical, IR, electron spin resonance and conductivity properties of a-Ge1-xCx:H with a-Ge:H and a-Ge thin films prepared by r.f. sputtering[J]. Thin Solid Films.1991,198(1-2):75-84.
[20] 许小红, 武海顺, 张富强, 等. 反应溅射制备AlN薄膜中沉积速率的研究[J]. 稀有金属材料与工程, 2002(3): 208-211.
[21] 许小亮, 王烨, 赵亚丽, 等. 磁控溅射法制备的纳米金薄膜的工艺条件和结构分析[J]. 功能材料, 2006(8): 1216-1219.
[22] 郭俊婷, 徐阳. 磁控溅射法沉积纳米Cu薄膜的性能研究[J]. 功能材料, 2015, 46(5): 5123-5127.
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